Benzyl Alcohol to Benzaldehyde oxidation w/Nitric acid - 92%+ yield. Concerning the benzyl alcohol oxidation to benzaldehyde in the absence of alkali, early reports deal principally with liquid phase reactions which rarely reach the total conversion and show a selectivity in the range of 90–100% in spite of a quite low TOF , , , , . - Free download as PDF File (.pdf), Text File (.txt) or read online for free. It even scales well (tested with 1.5 liters of Benzyl alcohol in a single run).

Certified DIY. Benzyl alcohol is an easily obtainable chemical, it is a common paint remover. Another thing: MnO2 is the major product of KMnO4 oxidation, and even that can oxidize benzyl alcohol to benzaldehyde.

So take that into consideration when calculating stoichiometry. I believe the way I've done it is by having the KMnO4 in an aqueous layer and just stirred vigorously with low heat. This method works great and yields are always good - 92% and up. mechanism for the oxidation of benzyl alcohol using nitric acid is proposed, showing the reversible formation of benzyl nitrite and its irreversible decomposition to benzaldehyde…

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